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277

Materials Science and Mechanics of Materials

Measurement, Redistribution and Relaxations of Residual Stress

Residual stresses, typically

acting on different length

scales depending on the

mechanisms they originate

from, can be beneficial or

detrimental for the material and

component performance. As a

consequence of compressive

macroscopic stresses near the

surface of a component, the

accumulation of micro-cracks

can be reduced and the life-

time of the component can be

extended. In contrast, tensile

macroscopic stresses can

lead to spontaneous cracking

which can reduce strength and

toughness.

A redistribution of residual

stress may result either from

the removal of portions of a

workpiece during machining

or from stress relaxation in

the material due to diffusion

processes and plays a central

role for most experimental

techniques applied for residual

stress analysis. Residual stress redistributions may lead

to undesired distortions of the whole component during

machining to its final shape or during the component’s

operating life. The macroscopic temperature-dependent

damping behavior of the material can provide important

information about the governing (microscopic) diffusion

processes, as it results from energy dissipation by internal

friction caused by (thermally activated) migration of crystal

lattice defects during loading/deformation.

In this context, research activities of WKM focus on

investigations of (residual) stress redistributions both on

macroscopic and microscopic scales as well as on the

identification of the underlying microscopic mechanisms.

This includes the application and further development

of experimental techniques involving diffraction and

mechanical methods. To investigate the diffusion pro-

cesses governing residual stress relaxation, the macro-

scopic damping behavior of the materials is investigated

by dynamic mechanical spectroscopy using an instru-

mented torsion pendulum and the impulse excitation

method.

Besides the semi-destructive hole drilling method, which

is an effective way of determining near-surface residual

stresses, dissection/slitting methods like boring of cylin-

ders are applied to analyze

axisymmetric residual stress

distributions in cylindrical

specimens. In most cases, an

accompanying residual stress

analysis via X-ray diffraction

on the specimen’s surface is

promising.

Neutron diffraction offers

the possibility of a spatially-

resolved, phase-specific and

non-destructive residual stress

analysis up to several centi­

meters below the component’s

surface. In-situ neutron

diffraction experiments play

a central role within the

research activities of WKM

focusing on the evolution of

the intergranular and inter-

phase microstrains of different

nickel-base superalloys

(Inconel 718 and Haynes 282)

during loading and unloading

at room temperature and at elevated temperatures. Haynes

282, due to its good creep strength, thermal stability and

weldability, is developed for avian and land-based appli-

cations and exhibits a low diversity of precipitates and a

small lattice misfit, opening up the possibility of an in-depth

study on the micromechanics of the anomalous yielding

effect. A complementary rigorous characterization of both

microstructural aspects and their kinetics on different

length scales is accomplished by light- and electronmi-

croscopy (SEM/TEM), 3D-atomprobe tomography, small

angle neutron scattering, as well as X-ray diffraction. These

combined experimental techniques will help to identify the

mechanisms governing the different microstrain-accumula-

tion behavior of these alloys.

Project

■■

Entwicklung von Typ II Eigendehnungen in Abhängig-

keit der Mikrostruktur in Nickelbasislegierungen (DFG,

KR3687/3-1)

Partners

■■

Karlsruher Institut für Technologie, Institut für Ange-

wandte Materialien – Werkstoffkunde, Engelbert-

Arnold-Str. 4, 76131 Karlsruhe

■■

Forschungs-Neutronenquelle Heinz Maier-Leibnitz

(FRM II), Technische Universität München, Lichtenberg-

str. 1, 85748 Garching

Characterization of the

axisymmetric residual stress

distribution in a cylindrical

specimen by WEDM (wire

electrical discharge machining)

assisted dissection. During

continuous material removal

on the inner cylindrical surface

via WEDM the strain relaxation

is simultaneously recorded by

strain gages mounted on the

lateral surface of the specimen.

(Source: WKM)

Semi-automatic residual

stress measurement via X-ray

diffraction (d-sin²x measure-

ment mode, two symmetrically

positioned linear detectors,

backscatter geometry) on

the surface of a cylindrical

specimen. (Source: WKM)